Monday, June 19, 2017

SCS NMR Spectrometer Status Now

Updated 19 June 2017 (DLO):
Working Status of Spectrometers.
Monday - Friday, 9 a.m. to 5:30 p.m., just walk in.
After business hours, use your i-Card (swipe several times as needed).

Use Mnova Version 11.0.1 Only.

RAL Spectrometers (Check ChemFOM for Availability):
  • Carver-Bruker 500 CryoProbe (CB500) - Partially OK.  H-NMR and C-NMR and 2D NMR OK.  No other nuclei. Solvent suppression OK for H-NMR.  Part being order from Europe.  Time frame uncertain for full performance.
    • Ask a staff member for account registration, then a trained person in your group for automation instruction.  Be careful with 2D NMR set-up.
  • U500 - OK, but no spinning for now.
  • UI400 - OK. H, B-11, F, P only.  Spins OK.  No C-13.  Use LN2 bucket for cooling.
  • UI500NB - OK.  OK for all 1D and 2D NMR, but calibrate pw90 and T1 for protons using posted modification (very minor).
  • VXR500 - OK.  For H, C, P, F.  VT -60 to +80 C
  • SUNDS1 - OK.
  • Printers - Both OK.
Noyes Lab Spectrometers
  • UI300WB- OK; Reservations via Andre Sutrisno. 
  • UI600 - OK; Reservations via Lingyang Zhu.   
Chem Life Spectrometer
  • VNS750NB - OK; Reservations via Lingyang.  Currently in liquids NMR configuration.