Thursday, April 27, 2017

SCS NMR Spectrometer Status Now

Updated 27 Apr 2017 (DLO):
Working Status of Spectrometers.
Monday - Friday, 9 a.m. to 5:30 p.m., just walk in.
After business hours, use your i-Card (swipe several times as needed).

Use Mnova Version 10.0 Only.

RAL Spectrometers (Check ChemFOM for Availability):
  • Carver-Bruker 500 CryoProbe (CB500) - OK.
    • One Group running 500 samples in about 3-4 days; brief samples.
    • Ask a staff for account registration, then a trained person in your group for automation instruction.
  • U500 - OK.
  • UI400 - OK H-1 & C-13 only.  Spins OK.  No F-19, P-31, B-11.  Use LN2 bucket for cooling.  Some coursework activity. See posted schedules to plan ahead.
  • UI500NB - OK.  OK for all 1D and 2D NMR, but calibrate pw90 and T1 for protons using posted modification (very minor).
    • Now optimized for BioPak.
  • VXR500 - OK for H, C, P, F.  VT -60 to +80 C
  • SUNDS1 - OK.
  • Printers - Both OK.
Noyes Lab Spectrometers
  • UI300WB- OK; Reservations via Andre Sutrisno. 
  • UI600 - OK; Reservations via Lingyang Zhu.   
Chem Life Spectrometer
  • VNS750NB - OK; Reservations via Lingyang.  Currently in Liquids NMR configuration.  Changing to ssNMR configuration May 1 for about 3 weeks.